Atomic spectrometry updateX-ray fluorescence spectrometry
Identifieur interne : 000589 ( Main/Exploration ); précédent : 000588; suivant : 000590Atomic spectrometry updateX-ray fluorescence spectrometry
Auteurs : Margaret Westreview Coordinator [Royaume-Uni] ; Andrew T. Ellis [États-Unis] ; Philip J. Potts [Royaume-Uni] ; Christina Streli [Autriche] ; Christine Vanhoof [Belgique] ; Dariusz Wegrzynek [Pologne] ; Peter Wobrauschek [Autriche]Source :
- Journal of Analytical Atomic Spectrometry [ 0267-9477 ] ; 2010.
Abstract
This comprehensive review covers the latest published activities using XRF techniques. X-ray analytical equipment continues to be integrated with X-ray emission/diffraction/absorption techniques with the growing use of synchrotron radiation (SR) sources reflected in the literature. This integration trend was also prevalent in the development of small-scale laboratory equipment. X-ray detectors have advanced with pixellated systems, micro-calorimeter types and the now established silicon drift detectors being readily used by many authors. Matrix correction and calibration procedures have developed to accommodate instrumental developments related to micro-beam and bulk analysis. SR-based micro-techniques for two and three dimensional imaging were reported in research activities in applications for clinical, biological, environmental and cultural heritage studies as well as investigations of extraterrestrial material. Sample preparation developments continue, especially for TXRF. The extension of TXRF to measure the angle dependence fluorescence signal (GI-XRF, XSW) showed increased interest with several groups applying the technique to depth profiling and thin layer analysis of nano-particles. More applications were reported this year for the reversed technique (GE-XRF) combining micro-beam analysis with surface sensitivity. Geochemical mapping of the moon is reported after space flight measurements used the Sun as a radiation source. The literature reflects increasing quantitative analysis using portable XRF with a welcomed growth in acceptance by the Food and Drug authorities and other applied users. This year's Update offers dietary delights for those who enjoy crab meat and an insight into the eating habits of elephants. Advice for gardeners contemplating a green roof is reported along with analysis of the wood treatments used in the manufacture of Stradivari and Guarneri violins. XRF has also played its part in the development of self-cleaning fabrics.
Url:
DOI: 10.1039/c005501h
Affiliations:
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X-ray analytical equipment continues to be integrated with X-ray emission/diffraction/absorption techniques with the growing use of synchrotron radiation (SR) sources reflected in the literature. This integration trend was also prevalent in the development of small-scale laboratory equipment. X-ray detectors have advanced with pixellated systems, micro-calorimeter types and the now established silicon drift detectors being readily used by many authors. Matrix correction and calibration procedures have developed to accommodate instrumental developments related to micro-beam and bulk analysis. SR-based micro-techniques for two and three dimensional imaging were reported in research activities in applications for clinical, biological, environmental and cultural heritage studies as well as investigations of extraterrestrial material. Sample preparation developments continue, especially for TXRF. The extension of TXRF to measure the angle dependence fluorescence signal (GI-XRF, XSW) showed increased interest with several groups applying the technique to depth profiling and thin layer analysis of nano-particles. More applications were reported this year for the reversed technique (GE-XRF) combining micro-beam analysis with surface sensitivity. Geochemical mapping of the moon is reported after space flight measurements used the Sun as a radiation source. The literature reflects increasing quantitative analysis using portable XRF with a welcomed growth in acceptance by the Food and Drug authorities and other applied users. This year's Update offers dietary delights for those who enjoy crab meat and an insight into the eating habits of elephants. Advice for gardeners contemplating a green roof is reported along with analysis of the wood treatments used in the manufacture of Stradivari and Guarneri violins. XRF has also played its part in the development of self-cleaning fabrics.</div></front></TEI><affiliations><list><country><li>Autriche</li><li>Belgique</li><li>Pologne</li><li>Royaume-Uni</li><li>États-Unis</li></country><region><li>Vienne (Autriche)</li></region><settlement><li>Vienne (Autriche)</li></settlement></list><tree><country name="Royaume-Uni"><noRegion><name sortKey="Westreview Coordinator, Margaret" sort="Westreview Coordinator, Margaret" uniqKey="Westreview Coordinator M" first="Margaret" last="Westreview Coordinator">Margaret Westreview Coordinator</name></noRegion><name sortKey="Potts, Philip J" sort="Potts, Philip J" uniqKey="Potts P" first="Philip J." last="Potts">Philip J. Potts</name></country><country name="États-Unis"><noRegion><name sortKey="Ellis, Andrew T" sort="Ellis, Andrew T" uniqKey="Ellis A" first="Andrew T." last="Ellis">Andrew T. Ellis</name></noRegion></country><country name="Autriche"><region name="Vienne (Autriche)"><name sortKey="Streli, Christina" sort="Streli, Christina" uniqKey="Streli C" first="Christina" last="Streli">Christina Streli</name></region><name sortKey="Wobrauschek, Peter" sort="Wobrauschek, Peter" uniqKey="Wobrauschek P" first="Peter" last="Wobrauschek">Peter Wobrauschek</name></country><country name="Belgique"><noRegion><name sortKey="Vanhoof, Christine" sort="Vanhoof, Christine" uniqKey="Vanhoof C" first="Christine" last="Vanhoof">Christine Vanhoof</name></noRegion></country><country name="Pologne"><noRegion><name sortKey="Wegrzynek, Dariusz" sort="Wegrzynek, Dariusz" uniqKey="Wegrzynek D" first="Dariusz" last="Wegrzynek">Dariusz Wegrzynek</name></noRegion></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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